Numerical optimization of the sintering process of dispersed electroerosion particles of the alloy VNZh 95
https://doi.org/10.22405/2226-8383-2021-22-3-298-310
Abstract
In this paper, the optimal parameters of the process of obtaining a heavy tungsten alloy by spark plasma sintering of the particles of the alloy VNZh 95 on the microhardness of the sintered
samples are determined by conducting a full factorial experiment of the type. The operating parameters of the spark plasma sintering unit were selected as factors: temperature, pressure,
and holding time, min. The optimal parameters of the installation operation were determined for the electroerosive material VZH 95, previously obtained in two working media: distilled water
and lighting kerosene. According to a series of experiments to determine the maximum value of the optimization parameter Y (microhardness), which amounted to: for samples obtained
from particles dispersed in water — 3498,6 MPa at 𝑇 = 1050∘C, a pressure of 𝑃 = 40 MPa and holding time 𝑡 = 10 min; for samples obtained from particles dispersed in kerosene — 2449,2 MPa at a temperature 𝑇 = 1200∘C, 𝑃 = 40 MPa and holding time 𝑡 = 5 min. The results of experimental studies of the composition, structure, and properties of heavy tungsten alloys made of electroerosion-dispersed particles of the VNJ 95 alloy obtained under optimal
conditions are presented below.
About the Authors
Ekaterina Vladimirovna AgeevaRussian Federation
candidate of technical sciences, associate professor
Evgeniy Viktorovich Ageev
Russian Federation
doctor of technical sciences, professor
Olga Vladimirovna Kuzovleva
Russian Federation
candidate of technical sciences, docent
Alexander Evgenievich Gvozdev
Russian Federation
doctor of engineering, professor
References
1. Levinson E.M. 1961, Electroerosion treatment of metals. Leningrad, Lenizdat. 184 p.
2. Burtsev V.A., Kalinin N.V., Luchinsky A.V. 1990, Electric explosion of conductors and its application in electrophysical installations. Moscow, Energoatomizdat. 288 p.
3. Gray V.S., Valevich V.V. 1999, «Preparation of highly dispersed metal powders method of electric explosion in the nitrogen of low pressure», Letters to the ZhTF, Vol.25, No.14, pp. 81-84.
4. Ageev E.V., Gadalov V.N., Semenikhin B.A., Ageeva E.V., Latypov R.A. 2010, «Obtaining wear-resistant powders from solid alloy waste», Procurement in mechanical engineering, No.12, рp. 39-44.
5. Ageev E.V., Gadalov V.N., Semenikhin B.A., Ageeva E.V., Latypov R.A. 2011, «X-ray Structural analysis of powders obtained by electroerosive dispersion of a hard alloy», Procurement in mechanical engineering, No.2, pp. 42-44.
6. Ageev E.V., Gadalov V.N., Semenikhin B.A., Ageeva E.V., Latypov R.A. 2011, «X-ray Spectral microanalysis of powder particles obtained by electroerosive dispersion of hard alloy»,
7. Strengthening technologies and coatings, No.2(74), pp. 13-16.
8. Ageev E.V., Semenikhin B.A., Ageeva E.V., Latypov RA. 2011, «Evaluation of the effectiveness of the use of hard-alloy powders obtained by electroerosive dispersion of solid-alloy waste in
9. the restoration and strengthening of parts with composite electroplating coatings», Hardening technologies and coatings, No.9(81), pp. 14-16.
10. Ageev E.V., Latypov R.A., Ageeva E.V. 2014, «Investigation of properties of electroerosive powders and hard alloy obtained from them by isostatic pressing and sintering», News of higher
11. educational institutions. Nonferrous metallurgy, No.6, pp. 51-55.
12. Ageeva E.V., Horakova N.M. Ageev E.V. 2014, «Morphology and elemental composition of copper electroerosion powders suitable for sintering», Bulletin of mechanical engineering, No.10, pp. 66-68.
13. Ageeva E.V., Ageev E.V., Vorobyov E.A. 2014, «X-ray Spectral microanalysis of a powder obtained from high-speed steel waste by electroerosive dispersion in kerosene», Bulletin of
14. mechanical engineering, No.11, pp. 71-72. 11. Ageeva E.V., Ageev E.V., Karpenko V.Yu. 2014, «X-ray Structural analysis of a powder
15. obtained from tungsten-containing waste by electroerosive dispersion in an aqueous medium»,
16. Bulletin of mechanical engineering, No.12, pp. 64-65.
17. Ageeva E.V., Horyakova N.M., Ageev E.V. 2014, «Investigation of the form and morphology of
18. electroerosive copper powders obtained from waste», Bulletin of mechanical engineering, No.8, pp. 73-75.
19. Ageeva E.V., Horyakova N.M., Ageev E.V. 2014, «Investigation of the size distribution of microparticles in powders obtained by electroerosive dispersion of copper waste», Bulletin of mechanical engineering, No.9, pp. 63-64.
20. Ageev E.V., Ageeva E.V., Vorobiev E.A. 2014, «Granulometric and phase compositions of powder obtained from tungsten-containing waste of tool materials by electroerosive dispersion in kerosene», Hardening technologies and coatings, No.4(112), pp. 11-14.
21. Ageeva E.V., Ageev E.V., Karpenko V.Yu. 2014, «Study of the form and elemental composition of a powder obtained from tungsten-containing waste of tool materials by electroerosive
22. dispersion in an aqueous medium», Hardening technologies and coatings, No.4(112), pp. 14- 17.
23. Horyakova N.M., Ageev E.V., Ageeva E.V. 2014, «Electroerosive copper powders for electroplating coatings», Strengthening technologies and coatings, No.4(112), pp. 18-20.
24. Ageeva E.V., Ageev E.V., Vorobyov E.A., Osminina A.S. 2014, «Obtaining wear-resistant coatings using electrodes from hard-alloy electroerosive powders and their research», Hardening
25. technologies and coatings, No.4(112), pp. 21-23.
26. Ageev E.V., Ageeva E.V., Karpenko V.Yu., Osminina A.S. 2014, «Obtaining hard alloy billets from powders obtained by electroerosive dispersion of tungsten-containing waste», Hardening technologies and coatings, No.4(112), pp. 24-27.
27. Ageeva E.V., Ageev E.V., Horyakova N.M. 2014, «Production of blanks from copper powders obtained by electroerosive dispersion of waste electrical copper and study of their properties», Science-Intensive technologies in mechanical engineering, No.10(40), pp. 10-13.
28. Ageeva E.V., Ageev E.V., Karpenko V.Yu. 2015, «Dimensional analysis of powder particles obtained from tungsten-containing waste by electroerosive dispersion in water», Bulletin of
29. mechanical engineering, No.3, pp. 45-46.
30. Ageeva E.V., Ageev E.V., Vorobiev E.A. 2015, «Analysis of the shape and morphology of powder particles obtained from tungsten-containing waste by electroerosive dispersion in kerosene», Bulletin of mechanical engineering, No.7, pp. 72-73.
31. Ageeva E.V., Latypov R.A., Ageev E.V., Altukhov A.Yu., Karpenko V.Yu. 2015, «Assessment of wear resistance of electric spark coatings obtained using high-speed steel electroerosive powders», News of higher educational institutions. Powder metallurgy and functional coatings, No.1, pp. 71-76.
32. Ageeva E.V., Latypov R.A., Ageev E.V., Altukhov A.Yu., Karpenko V.Yu. 2015, «Characteristics of electric spark coatings obtained by electrodes from high-speed steel electroerosive
33. powders», News of higher educational institutions. Powder metallurgy and functional coatings, No.2, pp. 62-65.
34. Ageeva E.V., Ageev E.V., Latypov R.A. 2015, «Evaluation of wear resistance of electric spark coatings obtained using high-speed steel electroerosive powders», News of higher educational
35. institutions. Powder metallurgy and functional coatings, No.3, p. 45.
36. Ageeva E.V., Horakova N.M. Pikalov, S.V., Ageev E.V. 2015, «Composition, structure and properties of copper spark erosion powder obtained in an environment of kerosene», News of
37. higher educational institutions. Powder metallurgy and functional coatings, No.4, pp. 4-8.
38. Holm R. 1961, Electrical contacts. Moscow, Foreign literature Publishing house. 464 p.
Review
For citations:
Ageeva E.V., Ageev E.V., Kuzovleva O.V., Gvozdev A.E. Numerical optimization of the sintering process of dispersed electroerosion particles of the alloy VNZh 95. Chebyshevskii Sbornik. 2021;22(3):298-310. (In Russ.) https://doi.org/10.22405/2226-8383-2021-22-3-298-310